List of Experiments / Activities
- List of Experiments (Any Ten Experiments)
- 1Setting Time of Cement Determine initial and final setting times of ordinary Portland cement using Vicat's apparatus; relate setting behaviour to hydration chemistry and w/c ratio
- 2Consistency of Cement Paste Determine the standard consistency of cement paste using Vicat's apparatus; understand its significance in mix design and workability
- 3Corrosion of Iron – Effect of Electrolyte Study the effect of NaCl, H2SO4, and distilled water on the rate of corrosion of iron nails; measure weight loss over time; relate to chloride-induced corrosion in concrete
- 4Effectiveness of Corrosion Inhibitors Study the inhibition of mild steel corrosion in HCl using organic inhibitors (e.g. aniline, thiourea); calculate inhibition efficiency; relate to protective coatings on rebars
- 5Determination of pH, TDS, and Conductivity of Water Measure pH, total dissolved solids (TDS), and electrical conductivity of given water samples using electrode meters; classify water suitability for construction use
- 6Determination of Total Hardness of Water Determine temporary and permanent hardness of water by EDTA titration method; relate to scaling in water pipes and quality of mixing water for concrete
- 7Estimation of Chloride Content in Water Determine chloride ion concentration in water samples by Mohr's method (argentometric titration); assess suitability of water for RCC construction
- 8Fineness of Cement by Sieve Analysis Determine fineness of cement using 90-micron IS sieve; relate fineness to rate of hydration, strength development, and heat of hydration in concrete
- 9Determination of Specific Gravity of Cement Determine specific gravity of cement using Le Chatelier's flask and kerosene; relate to concrete mix design calculations
- 10Viscosity of Adhesive / Polymer Coating Measure viscosity of given adhesive or polymer coating solution using Ostwald viscometer at different concentrations; relate to workability and adhesion in structural bonding applications
- 11Tensile Strength of Adhesive Bond Prepare lap-joint specimens bonded with epoxy or polymer adhesive; measure tensile shear strength; compare with reference standard; relate to FRP bonding in structural retrofitting
- 12Determination of COD of Waste Water Determine Chemical Oxygen Demand (COD) of a given wastewater sample by dichromate reflux method; assess organic pollution load relevant to construction site wastewater management
- Equipment / Chemicals Required
- •Vicat's apparatus, mould, glass plate
- •Analytical balance, weighing balance
- •pH meter, TDS meter, conductivity meter
- •Burette, pipette, conical flask, standard EDTA and AgNO3 solutions
- •Ostwald viscometer, thermostat water bath
- •Corrosion cell setup with salt bridge
- •Le Chatelier's flask
- •COD apparatus (reflux condenser, digestion flask)
- •Tensile testing machine or spring balance setup for adhesive bond test
Course Objectives
- To determine the chemical and physical properties of construction materials including cement and water
- To study corrosion phenomena and evaluate effectiveness of corrosion inhibitors
- To perform water quality analysis relevant to civil engineering applications
- To characterize sustainable building materials and study their chemical behaviour
- To evaluate adhesive strength and coating properties used in structural applications
Course Outcomes (COs)
After completion of the course student will be able to:
- CO1Determine setting time and consistency of cement and relate to hydration chemistryK3
- CO2Evaluate corrosion rate of iron and assess inhibitor efficiency for structural protectionK3
- CO3Perform water quality analysis and determine suitability of water for constructionK3
- CO4Characterize cement properties and relate to mix design for sustainable concreteK3
- CO5Measure viscosity and tensile strength of adhesives and coatings for structural applicationsK3
Suggested Textbooks / Reference Books
- Engineering Chemistry – Jain and Jain
- Concrete Technology – M.S. Shetty
- Water Supply Engineering – S.K. Garg Safety and General Instructions
- Students must wear lab coat and safety goggles at all times in the chemistry laboratory
- Handle all acids, alkalis, and oxidising agents with extreme care; use fume hood for volatile chemicals
- Dispose of chemical waste in designated containers as per lab safety guidelines
- Do not pipette by mouth; use rubber bulb or mechanical pipette fillers
- Wash hands thoroughly after every experiment; report any spillage or accident immediately
Official AKTU syllabus
This subject is on page 56, 57, 58, 59, 60 of the original AKTU PDF.